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By careful control of contamination levels, it is possible to conduct analyses at these low levels (12). The use of background subtraction software in this study has indicated to us that it must be used with caution, particularly at sample levels that are no more than 10 times the background. At these levels the variations in blanks can cause more problems than help. The precision and accuracy of replicate vapor phase microwave hydrolyses reported here is as good as that of 24 hr vapor phase hydrolyses.
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